Technology Process of Benzoyl chloride, 5-iodo-2,3-dimethoxy-
There total 11 articles about Benzoyl chloride, 5-iodo-2,3-dimethoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
N,N-dimethyl-formamide;
In
dichloromethane;
for 1h;
Ambient temperature;
DOI:10.1021/jo00018a048
- Guidance literature:
-
2,3-dimethoxybenzoic acid;
With
N-iodo-succinimide; trifluoroacetic acid;
In
acetonitrile;
for 48h;
Inert atmosphere;
Reflux;
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1016/j.tet.2017.04.028
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KMnO4; K2HPO4 / 2-methyl-propan-2-ol; H2O / 20 °C
2: SOCl2; DMF / toluene / Heating
With
potassium permanganate; dipotassium hydrogenphosphate; thionyl chloride; N,N-dimethyl-formamide;
In
water; toluene; tert-butyl alcohol;
1: Oxidation / 2: Substitution;
