(+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid

Base Information

Chemical Name:(+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid
CAS No.:184592-61-8
Molecular Formula:C₃₄H₂₇NO₁₁S
Molecular Weight:657.654
Hs Code.:

Synonyms:(+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid

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Chemical Property of (+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:969°C at 760 mmHg
Flash Point:539.8°C
Density:1.512g/cm³

Purity/Quality:

Safty Information:

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Technology Process of (+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid

There total 4 articles about (+-)-2-[[2,6-Dihydroxy-4-[[[3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)a mino]propyl]oxy]carbonyl]phenyl]carbonyl]-3-hydroxybenzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158585-06-9
4-(6-Benzyloxy-2-(benzyloxycarbonyl)benzoyl)-3,5-dibenzyloxybenzoic Acid

: 184592-61-8
(+/-)-2-({2,6-dihydroxy-4-[({3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 2 h / Ambient temperature

2: Et₃N, DMAP / CH₂Cl₂

3: TFA, H₂ / 20percent Pd(OH)2/C / ethanol; ethyl acetate / 760 Torr

With dmap; oxalyl dichloride; hydrogen; triethylamine; trifluoroacetic acid; palladium dihydroxide; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm960581w

Reference yield:

: 167832-93-1
3-Benzyloxy-2-(2,6-bis-benzyloxy-4-chlorocarbonyl-benzoyl)-benzoic acid benzyl ester

: 184592-61-8
(+/-)-2-({2,6-dihydroxy-4-[({3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, DMAP / CH₂Cl₂

2: TFA, H₂ / 20percent Pd(OH)2/C / ethanol; ethyl acetate / 760 Torr

With dmap; hydrogen; triethylamine; trifluoroacetic acid; palladium dihydroxide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm960581w

Reference yield:

: Carbonic acid benzyl ester 4-[3-hydroxy-2-(naphthalene-2-sulfonylamino)-propyl]-phenyl ester

: 184592-61-8
(+/-)-2-({2,6-dihydroxy-4-[({3-(4-hydroxyphenyl)-2-[(naphthylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, DMAP / CH₂Cl₂

2: TFA, H₂ / 20percent Pd(OH)2/C / ethanol; ethyl acetate / 760 Torr

With dmap; hydrogen; triethylamine; trifluoroacetic acid; palladium dihydroxide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm960581w