Technology Process of Carbamic acid,
[3,5-bis[[[2,3-bis(acetyloxy)propyl]amino]carbonyl]-2,4,6-triiodophenyl]-,
oxiranylmethyl ester
There total 5 articles about Carbamic acid,
[3,5-bis[[[2,3-bis(acetyloxy)propyl]amino]carbonyl]-2,4,6-triiodophenyl]-,
oxiranylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 6 h / Ambient temperature
2: dioxane; toluene / 15 h / 60 °C
3: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
With
pyridine;
phenylmercuric acetate;
In
1,4-dioxane; toluene;
DOI:10.1021/jo00085a023
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 74 percent / aq. potassium iododichloride / H2O / 18 h / 55 - 60 °C
2: 92 percent / thionyl chloride
3: N,N-dimethyl-acetamide / 16 h / Ambient temperature
4: pyridine / 6 h / Ambient temperature
5: dioxane; toluene / 15 h / 60 °C
6: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
With
pyridine; thionyl chloride; potassium dichloroiodate;
phenylmercuric acetate;
In
1,4-dioxane; N,N-dimethyl acetamide; water; toluene;
DOI:10.1021/jo00085a023
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / thionyl chloride
2: N,N-dimethyl-acetamide / 16 h / Ambient temperature
3: pyridine / 6 h / Ambient temperature
4: dioxane; toluene / 15 h / 60 °C
5: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
With
pyridine; thionyl chloride;
phenylmercuric acetate;
In
1,4-dioxane; N,N-dimethyl acetamide; toluene;
DOI:10.1021/jo00085a023
