Silane, ethenylmethylbis(phenylethynyl)-

Base Information

Chemical Name:Silane, ethenylmethylbis(phenylethynyl)-
CAS No.:136910-08-2
Molecular Formula:C₁₉H₁₆Si
Molecular Weight:272.422
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, ethenylmethylbis(phenylethynyl)-

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Technology Process of Silane, ethenylmethylbis(phenylethynyl)-

There total 1 articles about Silane, ethenylmethylbis(phenylethynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-70-9
Dichloromethylvinylsilane

: 536-74-3
phenylacetylene

: 136910-08-2
methyl[bis(phenylethynyl)]vinylsilane

Guidance literature:: With [{Ir(μ-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine; lithium iodide; at 90 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/om500320t

Reference yield: 99.0%

: 97-94-9
triethyl borane

: 136910-08-2
methyl[bis(phenylethynyl)]vinylsilane

: 1228317-14-3
(CH₃)(C₆H₅)2(CHCH₂)SiC₄(C₂H₅)B(C₂H₅)2

Guidance literature:: (Ar); NMR tube filled with silane deriv. and BEt3 in excess; sealed; kept at 100-120°C for 5 d; cooled in liq. N2; opened; vac. evapn.; detn. by NMR;
DOI:10.1515/znb-2009-1002

Reference yield: 95.0%

: 52102-17-7
9-ethyl-9-borabicyclo[3.3.1]nonane

: 136910-08-2
methyl[bis(phenylethynyl)]vinylsilane

: 1228317-28-9
(CH₃)(CCC₆H₅)2SiCHCH₂B(C₂H₅)C₈H₁₄

Guidance literature:: (Ar); NMR tube filled with silane deriv. and borane deriv. in excess; sealed; kept at 120°C for 15 h; cooled in liq. N2; opened; vac. evapn. with heating at 60-70.deegree.C; detn. by NMR;
DOI:10.1515/znb-2009-1002