3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl ester
CAS No.:136941-44-1
Molecular Formula:C₂₇H₂₇N₃O₉S
Molecular Weight:569.592
Hs Code.:
Mol file:136941-44-1.mol

3,5-Pyridinedicarboxylic acid,
1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-,
2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl
ester

Synonyms:

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl ester

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 143093-33-8
isopropyl β-aminocrotonate

: 141294-03-3
2-[1-(3-Nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid 2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl ester

: 136941-44-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: In ethanol; for 10h; Heating;
DOI:10.1021/jm00091a008

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 136941-44-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 70 percent / ethanol / 10 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008

Reference yield:

: 113658-92-7
2-(1,1,3-trioxo-2,3-dihydro-1,2-benzisothiazol-2-yl)ethyl acetylacetate

: 136941-44-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 70 percent / ethanol / 10 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008