3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl ester
CAS No.:136941-79-2
Molecular Formula:C₂₈H₂₉N₃O₁₀S
Molecular Weight:599.618
Hs Code.:
Mol file:136941-79-2.mol

3,5-Pyridinedicarboxylic acid,
1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-,
3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl
ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 3-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)propyl 2-methoxyethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 143093-34-9
(E)-3-Amino-but-2-enoic acid 2-methoxy-ethyl ester

: 141294-08-8
2-[1-(2-Nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid 3-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-propyl ester

: 136941-79-2
2,6-Dimethyl-5-(2-methoxyethoxycarbonyl)-4-(2-nitrophenyl)-1,4-dihydropyridine-3-carboxylic acid-3-[N-(1,2-benzisothiazolyl-3(2H)one-1,1-dioxide)]-propylester

Guidance literature:: In ethanol; for 18h; Heating;
DOI:10.1021/jm00091a008

Reference yield: 22.0%

: 136941-79-2
2,6-Dimethyl-5-(2-methoxyethoxycarbonyl)-4-(2-nitrophenyl)-1,4-dihydropyridine-3-carboxylic acid-3-[N-(1,2-benzisothiazolyl-3(2H)one-1,1-dioxide)]-propylester

Guidance literature:

Reference yield:

: 147701-47-1
3-Oxo-butyric acid 3-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-propyl ester

: 136941-79-2
2,6-Dimethyl-5-(2-methoxyethoxycarbonyl)-4-(2-nitrophenyl)-1,4-dihydropyridine-3-carboxylic acid-3-[N-(1,2-benzisothiazolyl-3(2H)one-1,1-dioxide)]-propylester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 22 percent / ethanol / 18 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008