3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester
CAS No.:136941-95-2
Molecular Formula:C₂₈H₂₉N₃O₉S
Molecular Weight:583.619
Hs Code.:
Mol file:136941-95-2.mol

3,5-Pyridinedicarboxylic acid,
1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl
2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(2-nitrophenyl)-, 1,1-dimethylethyl 2-(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 856427-32-2
tert-butyl (2E)-3-aminobut-2-enoate

: 141294-12-4
2-[1-(2-Nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid 2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl ester

: 136941-95-2
2,6-Dimethyl-4-(2-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-tert-butyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: In ethanol; for 12h; Heating;
DOI:10.1021/jm00091a008

Reference yield:

: 113658-92-7
2-(1,1,3-trioxo-2,3-dihydro-1,2-benzisothiazol-2-yl)ethyl acetylacetate

: 136941-95-2
2,6-Dimethyl-4-(2-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-tert-butyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 57 percent / ethanol / 12 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 136941-95-2
2,6-Dimethyl-4-(2-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-tert-butyl ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 57 percent / ethanol / 12 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008