Technology Process of 6-Octenoic acid, 5-(benzoyloxy)-7-methyl-, ethyl ester, (S)-
There total 6 articles about 6-Octenoic acid, 5-(benzoyloxy)-7-methyl-, ethyl ester, (S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: K2CO3 / ethanol / 8 h / Ambient temperature
2: pyridine / 4 h / 0 °C
With
pyridine; potassium carbonate;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 42 percent / benzene / 4 h / Ambient temperature; Irradiation
2: K2CO3 / ethanol / 8 h / Ambient temperature
3: pyridine / 4 h / 0 °C
With
pyridine; potassium carbonate;
In
ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 95 percent / DMSO, oxalyl chloride / CH2Cl2 / 0.25 h / -70 - -60 °C
2: 65 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 20 h / Ambient temperature
3: 93 percent / 57percent HI, water / acetone / 4 h / Ambient temperature
4: 92 percent / α,α'-azoisobutyronitrile, tributyltin hydride / benzene / 0.5 h / Ambient temperature
5: 42 percent / benzene / 4 h / Ambient temperature; Irradiation
6: K2CO3 / ethanol / 8 h / Ambient temperature
7: pyridine / 4 h / 0 °C
With
pyridine; oxalyl dichloride; azobisisobutyronitrile; water; hydrogen iodide; tri-n-butyl-tin hydride; potassium carbonate; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; acetone; benzene;