2-Propeneperoxoic acid, 3-phenyl-, 1-methoxy-1-methylethyl ester, (E)-

Base Information

• Chemical Name: 2-Propeneperoxoic acid, 3-phenyl-, 1-methoxy-1-methylethyl ester, (E)-
• CAS No.: 137846-27-6
• Molecular Formula: C13H16O4
• Molecular Weight: 236.268
• Mol file: 137846-27-6.mol

Synonyms:

Chemical Property of 2-Propeneperoxoic acid, 3-phenyl-, 1-methoxy-1-methylethyl ester, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-Propeneperoxoic acid, 3-phenyl-, 1-methoxy-1-methylethyl ester, (E)-

There total 1 articles about 2-Propeneperoxoic acid, 3-phenyl-, 1-methoxy-1-methylethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-hydroperoxy-2-methoxypropane (10027-74-4) + (E)-3-phenylacrylic acid (140-10-3) → 2-methoxyprop-2-yl (E)-3-phenyl-2-peroxypropenoate (137846-27-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1021/jo00029a043

Reference yield: 48.0%

2-methoxyprop-2-yl (E)-3-phenyl-2-peroxypropenoate (137846-27-6) → phenyl-2-peroxypropenoic acid (137846-29-8)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; acetic acid;

DOI:10.1021/jo00029a043

upstream raw materials:

2-hydroperoxy-2-methoxypropane

(E)-3-phenylacrylic acid

Downstream raw materials:

phenyl-2-peroxypropenoic acid

Refernces