Technology Process of Benzoic acid, 2-[(3,5-dimethoxyphenyl)methyl]-6-methoxy-4-methyl-
There total 4 articles about Benzoic acid, 2-[(3,5-dimethoxyphenyl)methyl]-6-methoxy-4-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuric acid; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
at 45 ℃;
for 6h;
under 3750.3 Torr;
DOI:10.1007/BF00811474
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) tetramethylethylenediamine, sec-butyl lithium / 1) THF, pentane, -80 deg C, 20 min, 2) -80 deg C, 20 min
2: p-toluenesulfonic acid / toluene / 2 h / Ambient temperature
3: 96 percent / conc. H2SO4, H2 / 10percent Pd/C / tetrahydrofuran / 6 h / 45 °C / 3750.3 Torr
With
N,N,N,N,-tetramethylethylenediamine; sulfuric acid; hydrogen; sec.-butyllithium; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; toluene;
DOI:10.1007/BF00811474
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) tetramethylethylenediamine, sec-butyl lithium / 1) THF, pentane, -80 deg C, 20 min, 2) -80 deg C, 20 min
2: p-toluenesulfonic acid / toluene / 2 h / Ambient temperature
3: 96 percent / conc. H2SO4, H2 / 10percent Pd/C / tetrahydrofuran / 6 h / 45 °C / 3750.3 Torr
With
N,N,N,N,-tetramethylethylenediamine; sulfuric acid; hydrogen; sec.-butyllithium; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; toluene;
DOI:10.1007/BF00811474
