1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide

Base Information

Chemical Name:1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide
CAS No.:54648-89-4
Molecular Formula:C18H18N4OS
Molecular Weight:338.4267
Hs Code.:
DSSTox Substance ID:DTXSID50203084

Synonyms:BRN 4551332;1H-INDOLE-3-ACETIC ACID, 2-METHYL-, 2-((PHENYLAMINO)THIOXOMETHYL)HYDRAZIDE;2-Methyl-1H-indole-3-acetic acid 2-((phenylamino)thioxomethyl)hydrazide;54648-89-4;DTXSID50203084;LS-82211

Suppliers and Price of 1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.348g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:338.12013238
Heavy Atom Count:24
Complexity:452

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C2=CC=CC=C2N1)CC(=O)NNC(=S)NC3=CC=CC=C3

Technology Process of 1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide

There total 6 articles about 1H-Indole-3-acetic acid, 2-methyl-, 2-((phenylamino)thioxomethyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 21909-51-3
2-(2-methyl-1H-indol-3-yl)acetohydrazide

: 103-72-0
phenyl isothiocyanate

: 54648-89-4
1-(2-methylindolyl-3-acetyl)-4-phenylthiosemicarbazide

Guidance literature:: In ethanol; Heating;

Reference yield:

: 1912-43-2
2-methyl-3-indoleacetic acid

: 54648-89-4
1-(2-methylindolyl-3-acetyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / K₂CO₃ / dimethylformamide / 10 h / Ambient temperature

2: 73 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

3: 78 percent / ethanol / 0.5 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0014-827X(98)00024-X

Reference yield:

: 78564-10-0
2-methylindole-3-acetic acid methyl ester

: 54648-89-4
1-(2-methylindolyl-3-acetyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

2: 78 percent / ethanol / 0.5 h / Heating

With hydrazine hydrate; In ethanol;
DOI:10.1016/S0014-827X(98)00024-X