(2-Iodo-3,4-dimethoxyphenyl)methanol

Base Information

Chemical Name:(2-Iodo-3,4-dimethoxyphenyl)methanol
CAS No.:138490-97-8
Molecular Formula:C9H11IO3
Molecular Weight:294.089
Hs Code.:
DSSTox Substance ID:DTXSID401294703
Mol file:138490-97-8.mol

Synonyms:(2-iodo-3,4-dimethoxyphenyl)methanol;138490-97-8;DTXSID401294703;2-Iodo-3,4-dimethoxybenzenemethanol;(2-iodo-3,4-dimethoxy-phenyl)-methanol

Suppliers and Price of (2-Iodo-3,4-dimethoxyphenyl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (2-Iodo-3,4-dimethoxyphenyl)methanol

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:293.97529
Heavy Atom Count:13
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)CO)I)OC

Technology Process of (2-Iodo-3,4-dimethoxyphenyl)methanol

There total 3 articles about (2-Iodo-3,4-dimethoxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 138490-95-6
2-iodo-3,4-dimethoxybenzaldehyde

: 138490-97-8
(2-iodo-3,4-dimethoxyphenyl)methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 40 ℃; for 3h;
DOI:10.1021/jm00081a007

Reference yield:

: 138490-94-5
2-iodoisovanillin

: 138490-97-8
(2-iodo-3,4-dimethoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / potassium carbonate / acetone / 6 h / Heating

2: 83 percent / sodium borohydride / tetrahydrofuran / 3 h / 40 °C

With sodium tetrahydroborate; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1021/jm00081a007

Reference yield:

: 621-59-0
isovanillin

: 138490-97-8
(2-iodo-3,4-dimethoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine, iodine monochloride / dioxane / 144 h / Ambient temperature

2: 85 percent / potassium carbonate / acetone / 6 h / Heating

3: 83 percent / sodium borohydride / tetrahydrofuran / 3 h / 40 °C

With pyridine; sodium tetrahydroborate; Iodine monochloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; acetone;
DOI:10.1021/jm00081a007