3-(1H-Indol-3-ylmethyl)-6-methyl-2,5-piperazinedione

Base Information

• Chemical Name: 3-(1H-Indol-3-ylmethyl)-6-methyl-2,5-piperazinedione
• CAS No.: 26384-48-5
• Molecular Formula: C₁₄H₁₅N₃O₂
• Molecular Weight: 257.292
• Mol file: 26384-48-5.mol

Synonyms:2,5-Piperazinedione,3-(indol-3-ylmethyl)-6-methyl- (6CI); Cyclo(alanyltryptophyl)

Chemical Property of 3-(1H-Indol-3-ylmethyl)-6-methyl-2,5-piperazinedione

Chemical Property:

• PSA: 73.99000
• LogP: 1.37110

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(1H-Indol-3-ylmethyl)-6-methyl-2,5-piperazinedione

There total 36 articles about 3-(1H-Indol-3-ylmethyl)-6-methyl-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Boc-Ala-Trp-OMe (207349-24-4) → (3S,6S)-3-(3'-indolylmethyl)-6-methylpiperazine-2,5-dione (17079-37-7,19943-35-2,22216-02-0,22216-03-1,22839-21-0,22839-22-1,22839-23-2,26384-48-5)

Guidance literature:

at 200 ℃;

DOI:10.1016/S0957-4166(98)00068-8

Reference yield: 100.0%

(R)-2-((S)-2-tert-Butoxycarbonylamino-propionylamino)-3-(1H-indol-3-yl)-propionic acid methyl ester (207349-42-6) → cyclo-D-Trp-L-Ala (17079-37-7,19943-35-2,22216-02-0,22216-03-1,22839-21-0,22839-22-1,26384-48-5,22839-23-2)

Guidance literature:

at 200 ℃;

DOI:10.1016/S0957-4166(98)00068-8

Reference yield: 100.0%

(S)-2-((R)-2-tert-Butoxycarbonylamino-propionylamino)-3-(1H-indol-3-yl)-propionic acid methyl ester (207349-25-5) → Cyclo-(L)-Trp-(D)-Ala (17079-37-7,19943-35-2,22216-02-0,22216-03-1,22839-21-0,22839-22-1,22839-23-2,26384-48-5)

Guidance literature:

at 200 ℃;

DOI:10.1016/S0957-4166(98)00068-8

upstream raw materials:

DL-alanine-DL-tryptophan

D-alanyl-L-tryptophan methyl ester

(S)-tryptophan methyl ester hydrochloride

Z-D-Ala-L-Trp-OMe

Downstream raw materials:

C₂₂H₁₈BrF₃N₄O₃

C₂₀H₁₉N₃O₂

C₂₀H₁₉N₃O₂

(3R,6S)-1-(o-Azidobenzoyl)-3-(3-indolylmethyl)-6-methyl-2,5-piperazinedione

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