4-Bromo-4'-decyloxybiphenyl

Base Information

Chemical Name:4-Bromo-4'-decyloxybiphenyl
CAS No.:138567-31-4
Molecular Formula:C22H29BrO
Molecular Weight:389.376
Hs Code.:
DSSTox Substance ID:DTXSID10443262
Wikidata:Q82260999

Synonyms:4-Bromo-4'-decyloxybiphenyl;138567-31-4;SCHEMBL7697448;DTXSID10443262;VILGWIYOEOBZFI-UHFFFAOYSA-N

Suppliers and Price of 4-Bromo-4'-decyloxybiphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Bromo-4'-decyloxybiphenyl

Chemical Property:

XLogP3:8.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:11
Exact Mass:388.14018
Heavy Atom Count:24
Complexity:290

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCOC1=CC=C(C=C1)C2=CC=C(C=C2)Br

Technology Process of 4-Bromo-4'-decyloxybiphenyl

There total 2 articles about 4-Bromo-4'-decyloxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 112-29-8
1-bromo dodecane

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 138567-31-4
4-bromo-4'-decyloxybiphenyl

Guidance literature:: With potassium carbonate; potassium iodide; In butanone;

Reference yield:

: 112-29-8
1-bromo dodecane

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 78-93-3
butanone

: 138567-31-4
4-bromo-4'-decyloxybiphenyl

Guidance literature:: With potassium carbonate;

Reference yield:

: 138567-31-4
4-bromo-4'-decyloxybiphenyl

: 159659-38-8
3-(4'-Decyloxy-biphenyl-4-yl)-2-methyl-cyclopent-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLI; triisopropylborate / hexane; tetrahydrofuran / 16 h / -78 - 20 °C

1.2: HCl / hexane; tetrahydrofuran; H₂O / 1 h / 20 °C

2.1: 98 percent / Pd(PPh₃)4; Na₂CO₃ / ethanol; H₂O; benzene / 16 h / Heating

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Triisopropyl borate; sodium carbonate; In tetrahydrofuran; ethanol; hexane; water; benzene;
DOI:10.1016/S0040-4020(03)00620-3