2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)-

Base Information

• Chemical Name: 2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)-
• CAS No.: 1830-77-9
• Molecular Formula: C22H17 N O2
• Molecular Weight: 327.382
• European Community (EC) Number: 217-387-9
• NSC Number: 50652
• UNII: 4YC1P4O512
• DSSTox Substance ID: DTXSID0062008
• Nikkaji Number: J7.790I
• Wikidata: Q81989789
• Mol file: 1830-77-9.mol

Synonyms:Naphtanilide GR;1830-77-9;Naphthol AS-GR;2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)-;Amarthol AS-GR;Tulathol AS GR;2-Anthro-o-toluidide, 3-hydroxy-;C.I. Azoic Coupling Component 36;3-hydroxy-N-(2-methylphenyl)anthracene-2-carboxamide;C.I. 37585;3-Hydroxy-2'-methylanthracene-2-carboxanilide;3-Hydroxy-2-anthro-o-toluidide;4YC1P4O512;EINECS 217-387-9;NSC 50652;NSC-50652;C22H17NO2;Oprea1_378946;UNII-4YC1P4O512;3-hydroxy-N-(2-methylphenyl)-2-Anthracenecarboxamide;SCHEMBL5681508;DTXSID0062008;NSC50652;C.I.37585;FT-0735443;2-HYDROXY-3-ANTHRACENECARBOXYLIC ACID O-TOLUIDIDE

Chemical Property of 2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)-

Chemical Property:

• Vapor Pressure: 5.04E-10mmHg at 25°C
• Boiling Point: 484.8°C at 760 mmHg
• Flash Point: 247°C
• PSA: 49.33000
• Density: 1.303g/cm³
• LogP: 5.33230
• XLogP3: 5.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 327.125928785
• Heavy Atom Count: 25
• Complexity: 479

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CC=C1NC(=O)C2=CC3=CC4=CC=CC=C4C=C3C=C2O

Technology Process of 2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)-

There total 1 articles about 2-Anthracenecarboxamide, 3-hydroxy-N-(2-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxy-3-anthranoic acid (6295-44-9) + o-toluidine (95-53-4) → 3-hydroxy-anthracene-2-carboxylic acid o-toluidide (1830-77-9)

Guidance literature:

With toluene; anschliessend Erhitzen mit Phosphor(III)-chlorid;

Reference yield:

3-hydroxy-anthracene-2-carboxylic acid o-toluidide (1830-77-9) → Phosphoric acid mono-(3-o-tolylcarbamoyl-anthracen-2-yl) ester (2616-73-1)

Guidance literature:

With phosphorus pentachloride; In 1,4-dioxane; at 50 ℃; for 1h;

DOI:10.1021/ac00080a022

Reference yield:

2,3-Dichloro-1,4-naphthoquinone (117-80-6) + 3-hydroxy-anthracene-2-carboxylic acid o-toluidide (1830-77-9) → 9,14-dioxo-9,14-dihydro-anthra[2,1-b]naphtho[2,3-d]furan-7-carboxylic acid o-toluidide (25082-85-3)

Guidance literature:

With pyridine;

upstream raw materials:

2-hydroxy-3-anthranoic acid

o-toluidine

Downstream raw materials:

9,14-dioxo-9,14-dihydro-anthra[2,1-b]naphtho[2,3-d]furan-7-carboxylic acid o-toluidide

Phosphoric acid mono-(3-o-tolylcarbamoyl-anthracen-2-yl) ester

Refernces