Technology Process of Benzenebutanoic acid, 4-[(2-chloroethyl)sulfinyl]-
There total 6 articles about Benzenebutanoic acid, 4-[(2-chloroethyl)sulfinyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
tert-butyl alcohol;
for 5h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) MeSNa / 1.) HMPA, 100 deg C, 6 h, 2.) 80 deg C, 2 h
2: 52 percent / NaIO4 / methanol; H2O / 24 h / 0 °C
3: 94 percent / aqueous HCl (2 mol dm-3) / acetone / 48 h / Heating
4: 48 percent / aqueous NaClO2 (23.2 mmol dm-3), aqueous NaH2PO4 (23.2 mmol dm-3), 2-methylbut-2-ene / 2-methyl-propan-2-ol / 5 h / Ambient temperature
With
hydrogenchloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; mesna;
In
methanol; water; acetone; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / aqueous HCl (2 mol dm-3) / acetone / 48 h / Heating
2: 48 percent / aqueous NaClO2 (23.2 mmol dm-3), aqueous NaH2PO4 (23.2 mmol dm-3), 2-methylbut-2-ene / 2-methyl-propan-2-ol / 5 h / Ambient temperature
With
hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
acetone; tert-butyl alcohol;