1,3-Dioxane-2-propanol, a-[4-(methylthio)phenyl]-

Base Information

Chemical Name:1,3-Dioxane-2-propanol, a-[4-(methylthio)phenyl]-
CAS No.:138793-02-9
Molecular Formula:C₁₄H₂₀O₃S
Molecular Weight:268.377
Hs Code.:
Mol file:138793-02-9.mol

Synonyms:

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Chemical Property of 1,3-Dioxane-2-propanol, a-[4-(methylthio)phenyl]-

Chemical Property:

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Technology Process of 1,3-Dioxane-2-propanol, a-[4-(methylthio)phenyl]-

There total 1 articles about 1,3-Dioxane-2-propanol, a-[4-(methylthio)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33884-43-4
2-(2-Bromoethyl)-1,3-dioxane

: 3446-89-7
4-(Methylthio)benzaldehyde

: 138793-02-9
2-<3-hydroxy-3-(p-methylthiophenyl)propyl>-1,3-dioxane

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) THF, 0 deg C, 10 min, 2. a) THF, reflux, b) 0 deg C, 2 h;

Reference yield:

: 138793-02-9
2-<3-hydroxy-3-(p-methylthiophenyl)propyl>-1,3-dioxane

: 138793-07-4
4-butanal

Guidance literature:: Multi-step reaction with 4 steps

1: 1. a) triethyl amine, b) methanesulphonyl chloride, 2.) LiAlH₄ / 1. a) CH₂Cl₂, 0 deg C, 30 min, b) r.t., 30 min, c) CH₂Cl₂, -5 deg C, 3 h, 2.) r.t., 2 h

2: 1.) MeSNa / 1.) HMPA, 100 deg C, 6 h, 2.) 80 deg C, 2 h

3: 52 percent / NaIO₄ / methanol; H₂O / 24 h / 0 °C

4: 94 percent / aqueous HCl (2 mol dm^-3) / acetone / 48 h / Heating

With hydrogenchloride; sodium periodate; lithium aluminium tetrahydride; mesna; methanesulfonyl chloride; triethylamine; In methanol; water; acetone;

Reference yield:

: 138793-02-9
2-<3-hydroxy-3-(p-methylthiophenyl)propyl>-1,3-dioxane

: 138793-01-8
4-butanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1. a) triethyl amine, b) methanesulphonyl chloride, 2.) LiAlH₄ / 1. a) CH₂Cl₂, 0 deg C, 30 min, b) r.t., 30 min, c) CH₂Cl₂, -5 deg C, 3 h, 2.) r.t., 2 h

2: 1.) MeSNa / 1.) HMPA, 100 deg C, 6 h, 2.) 80 deg C, 2 h

3: 52 percent / NaIO₄ / methanol; H₂O / 24 h / 0 °C

4: 94 percent / aqueous HCl (2 mol dm^-3) / acetone / 48 h / Heating

5: 48 percent / aqueous NaClO₂ (23.2 mmol dm^-3), aqueous NaH₂PO₄ (23.2 mmol dm^-3), 2-methylbut-2-ene / 2-methyl-propan-2-ol / 5 h / Ambient temperature

With hydrogenchloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; lithium aluminium tetrahydride; 2-methyl-but-2-ene; mesna; methanesulfonyl chloride; triethylamine; In methanol; water; acetone; tert-butyl alcohol;