1,3-Dioxane, 2-[3-[4-(methylthio)phenyl]propyl]-

Base Information

Chemical Name:1,3-Dioxane, 2-[3-[4-(methylthio)phenyl]propyl]-
CAS No.:138793-04-1
Molecular Formula:C₁₄H₂₀O₂S
Molecular Weight:252.378
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Dioxane, 2-[3-[4-(methylthio)phenyl]propyl]-

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Technology Process of 1,3-Dioxane, 2-[3-[4-(methylthio)phenyl]propyl]-

There total 2 articles about 1,3-Dioxane, 2-[3-[4-(methylthio)phenyl]propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138793-02-9
2-<3-hydroxy-3-(p-methylthiophenyl)propyl>-1,3-dioxane

: 138793-04-1
2-<3-(p-methylthiophenyl)propyl>-1,3-dioxane

Guidance literature:: With lithium aluminium tetrahydride; methanesulfonyl chloride; triethylamine; Yield given. Multistep reaction; 1. a) CH₂Cl₂, 0 deg C, 30 min, b) r.t., 30 min, c) CH₂Cl₂, -5 deg C, 3 h, 2.) r.t., 2 h;

Reference yield:

: 3446-89-7
4-(Methylthio)benzaldehyde

: 138793-04-1
2-<3-(p-methylthiophenyl)propyl>-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 0 deg C, 10 min, 2. a) THF, reflux, b) 0 deg C, 2 h

2: 1. a) triethyl amine, b) methanesulphonyl chloride, 2.) LiAlH₄ / 1. a) CH₂Cl₂, 0 deg C, 30 min, b) r.t., 30 min, c) CH₂Cl₂, -5 deg C, 3 h, 2.) r.t., 2 h

With lithium aluminium tetrahydride; magnesium; methanesulfonyl chloride; triethylamine;

Reference yield:

: 138793-04-1
2-<3-(p-methylthiophenyl)propyl>-1,3-dioxane

: 138793-07-4
4-butanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) MeSNa / 1.) HMPA, 100 deg C, 6 h, 2.) 80 deg C, 2 h

2: 52 percent / NaIO₄ / methanol; H₂O / 24 h / 0 °C

3: 94 percent / aqueous HCl (2 mol dm^-3) / acetone / 48 h / Heating

With hydrogenchloride; sodium periodate; mesna; In methanol; water; acetone;