Carbamic acid, [1-[[(4-benzoylphenyl)amino]acetyl]-5-[[(phenylmethoxy)carbonyl]amino] pentyl]-, 1,1-dimethylethyl ester, (S)-

Base Information

Chemical Name:Carbamic acid, [1-[[(4-benzoylphenyl)amino]acetyl]-5-[[(phenylmethoxy)carbonyl]amino] pentyl]-, 1,1-dimethylethyl ester, (S)-
CAS No.:138848-96-1
Molecular Formula:C33H39N3O6
Molecular Weight:573.689
Hs Code.:
Mol file:138848-96-1.mol

Synonyms:

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Chemical Property of Carbamic acid, [1-[[(4-benzoylphenyl)amino]acetyl]-5-[[(phenylmethoxy)carbonyl]amino] pentyl]-, 1,1-dimethylethyl ester, (S)-

Chemical Property:

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Technology Process of Carbamic acid, [1-[[(4-benzoylphenyl)amino]acetyl]-5-[[(phenylmethoxy)carbonyl]amino] pentyl]-, 1,1-dimethylethyl ester, (S)-

There total 1 articles about Carbamic acid, [1-[[(4-benzoylphenyl)amino]acetyl]-5-[[(phenylmethoxy)carbonyl]amino] pentyl]-, 1,1-dimethylethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.2%

: 1137-41-3,444317-48-0
(4-aminophenyl)(phenyl)methanone

: 82869-11-2
Boc-L-Lys(Z)-CH₂Cl

: 138848-96-1
Boc-Lys(Z)-4-benzoylanilinomethyl ketone

Guidance literature:: With sodium hydrogencarbonate; sodium iodide; In N,N-dimethyl-formamide; at 45 ℃; for 48h;
DOI:10.1248/cpb.39.2340

Reference yield:

: 138848-96-1
Boc-Lys(Z)-4-benzoylanilinomethyl ketone

: 138865-36-8
H-Lys(Z)-4-benzoylanilinomethyl ketone hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane;
DOI:10.1248/cpb.39.2340

Reference yield:

: 138848-96-1
Boc-Lys(Z)-4-benzoylanilinomethyl ketone

: 4-Aminomethyl-cyclohexanecarboxylic acid {(S)-5-amino-1-[2-(4-benzoyl-phenylamino)-acetyl]-pentyl}-amide; hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 5.6 N HCl / dioxane

2: Et₃N / CHCl₃; dimethylformamide / Ambient temperature

3: 37 percent / 25percent HBr/AcOH / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen bromide; acetic acid; triethylamine; In 1,4-dioxane; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.2340