(2α,17S,19E)-17-Acetoxy-19,20-didehydroajmalan-16-carboxylic acid methyl ester

Base Information

• Chemical Name: (2α,17S,19E)-17-Acetoxy-19,20-didehydroajmalan-16-carboxylic acid methyl ester
• CAS No.: 912-27-6
• Molecular Formula: C₂₄H₂₈N₂O₄
• Molecular Weight: 408.497
• Mol file: 912-27-6.mol

Synonyms:(6S,8aR,13aS,13bS)-8-Acetoxy-3-eth-(E)-ylidene-13-methyl-1,3,4,13,13a,13b-hexahydro-2H,6H-2,7-cyclo-6,8a-methano-pyrido[1',2':1,2]azepino[3,4-b]indole-7-carboxylic acid methyl ester;

Chemical Property of (2α,17S,19E)-17-Acetoxy-19,20-didehydroajmalan-16-carboxylic acid methyl ester

Chemical Property:

• Melting Point: 185°C
• PSA: 59.08000
• LogP: 2.27310

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: This carboline alkaloid has been isolated from Vinca difformis and V. minor and yields colourless prisms when crystallized from cydohexane. It is laevorotatory with [α]20D - 66° (c 0.52, CHCL3) or - 75° (c 1.0, CHCL3).

Technology Process of (2α,17S,19E)-17-Acetoxy-19,20-didehydroajmalan-16-carboxylic acid methyl ester

There total 1 articles about (2α,17S,19E)-17-Acetoxy-19,20-didehydroajmalan-16-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Vincamedin (912-27-6)

Guidance literature:

beim Behandeln von 2ξ-Hydroxy-vincamedin (s. Janot et al. Bl. 1962 1079 und Gosset, Diss, Paris 1963) mit KBH4 in Methanol (S: 678);

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