Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-

Base Information

Chemical Name:Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-
CAS No.:73942-30-0
Molecular Formula:C17H28ClNOSi
Molecular Weight:325.9488
Hs Code.:
DSSTox Substance ID:DTXSID00224648
Wikidata:Q83103281

Synonyms:BRN 6065506;Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-;2-(1-(p-Chlorophenyl)-1-silacyclohexyloxy)triethylamine;1-(4-Chlorphenyl)-1-(2-(dimethylamino)ethoxy)-silacyclohexan [German];73942-30-0;1-(4-Chlorphenyl)-1-(2-(dimethylamino)ethoxy)-silacyclohexan;C17H28ClNOSi;C17-H28-Cl-N-O-Si;DTXSID00224648;LS-157261

Suppliers and Price of Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-

Chemical Property:

Vapor Pressure:3.51E-06mmHg at 25°C
Boiling Point:386.6°Cat760mmHg
Flash Point:187.6°C
Density:1.04g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:325.1628687
Heavy Atom Count:21
Complexity:285

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCO[Si]1(CCCCC1)C2=CC=C(C=C2)Cl

Technology Process of Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)-

There total 5 articles about Triethylamine, 2-(1-(p-chlorophenyl)-1-silacyclohexyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 73942-27-5
1-(4-Chlorphenyl)-silacyclohexan

: 100-37-8
2-(Diethylamino)ethanol

: 73942-30-0
Silachlorphencyclane

Guidance literature:: With n-butyllithium; In hexane; for 6h;
DOI:10.1002/ardp.19803130206

Reference yield: 60.0%

: 72810-13-0
1-(4-Chlorphenyl)-1-chlor-silacyclohexan

: 100-37-8
2-(Diethylamino)ethanol

: 73942-30-0
Silachlorphencyclane

Guidance literature:: With triethylamine; In Petroleum ether; 1.) room temp., 1 h, 2.) reflux, 1 h;
DOI:10.1002/ardp.19803130206

Reference yield:

: 23708-48-7
pentamethylenebis(magnesium bromide)

: 73942-30-0
Silachlorphencyclane

Guidance literature:: Multi-step reaction with 3 steps

1: HSiCl₃ / diethyl ether / 1.) 20 deg C, 12 h, 2.) reflux, 4 h

2: diethyl ether / 1.) room temp., 6 h, 2.) reflux, 6 h

3: 83 percent / n-BuLi / hexane / 6 h

With n-butyllithium; trichlorosilane; In diethyl ether; hexane;
DOI:10.1002/ardp.19803130206