3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-, (1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl (tetrahydro-2H-pyran-2-yl)methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-, (1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl (tetrahydro-2H-pyran-2-yl)methyl ester
CAS No.:141294-18-0
Molecular Formula:C₂₉H₂₉N₃O₁₀S
Molecular Weight:611.629
Hs Code.:

3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-,
(1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl
(tetrahydro-2H-pyran-2-yl)methyl ester

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-, (1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl (tetrahydro-2H-pyran-2-yl)methyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-, (1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl (tetrahydro-2H-pyran-2-yl)methyl ester

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 2,6-dimethyl-4-(3-nitrophenyl)-, (1,1-dioxido-3-oxo-1,2-benzisothiazol-2(3H)-yl)methyl (tetrahydro-2H-pyran-2-yl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 136942-07-9
(E)-3-Amino-but-2-enoic acid tetrahydro-pyran-2-ylmethyl ester

: 141294-13-5
2-[1-(3-Nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid 1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-ylmethyl ester

: 141294-18-0
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(tetrahydro-pyran-2-ylmethyl) ester 5-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-ylmethyl) ester

Guidance literature:: In ethanol; for 10h; Heating;
DOI:10.1021/jm00091a008

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 141294-18-0
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(tetrahydro-pyran-2-ylmethyl) ester 5-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 65 percent / ethanol / 10 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008

Reference yield:

: 113658-93-8
(1,1,3-trioxo-2,3-dihydro-1,2-benzisothiazol-2-yl)methyl acetylacetate

: 141294-18-0
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(tetrahydro-pyran-2-ylmethyl) ester 5-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / acetic acid, piperidine / propan-2-ol / 1.) 40 deg C, 1 h, 2.) RT, 16 h, 3.) 0 deg C, 2 h

2: 65 percent / ethanol / 10 h / Heating

With piperidine; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00091a008