Benzoic acid, 4-iodo-, 2-oxoheptyl ester

Base Information

Chemical Name:Benzoic acid, 4-iodo-, 2-oxoheptyl ester
CAS No.:141339-62-0
Molecular Formula:C14H17IO3
Molecular Weight:360.192
Hs Code.:
Mol file:141339-62-0.mol

Synonyms:

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Chemical Property of Benzoic acid, 4-iodo-, 2-oxoheptyl ester

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Technology Process of Benzoic acid, 4-iodo-, 2-oxoheptyl ester

There total 3 articles about Benzoic acid, 4-iodo-, 2-oxoheptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 41055-92-9
1-chloro-2-heptanone

: 59786-02-6
potassium p-iodobenzoate

: 141339-62-0
4-Iodo-benzoic acid 2-oxo-heptyl ester

Guidance literature:: With tetrabutylammomium bromide; In benzene; for 3h; Heating;
DOI:10.1246/bcsj.65.631

Reference yield:

: 66720-07-8
tert-butyl 3-oxooctanoate

: 141339-62-0
4-Iodo-benzoic acid 2-oxo-heptyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / SO₂Cl₂ / CH₂Cl₂

2: 73 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

3: 69 percent / tetrabutylammonium bromide / benzene / 3 h / Heating

With sulfuryl dichloride; tetrabutylammomium bromide; toluene-4-sulfonic acid; In dichloromethane; benzene;
DOI:10.1246/bcsj.65.631

Reference yield:

: 141339-93-7
t-butyl 2-chloro-3-oxooctanoate

: 141339-62-0
4-Iodo-benzoic acid 2-oxo-heptyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 69 percent / tetrabutylammonium bromide / benzene / 3 h / Heating

With tetrabutylammomium bromide; toluene-4-sulfonic acid; In benzene;
DOI:10.1246/bcsj.65.631