Benzoic acid, 4-bromo-, 2-hydroxyheptyl ester, (S)-

Base Information

• Chemical Name: Benzoic acid, 4-bromo-, 2-hydroxyheptyl ester, (S)-
• CAS No.: 141339-69-7
• Molecular Formula: C₁₄H₁₉BrO₃
• Molecular Weight: 315.207
• Mol file: 141339-69-7.mol

Synonyms:

Chemical Property of Benzoic acid, 4-bromo-, 2-hydroxyheptyl ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-bromo-, 2-hydroxyheptyl ester, (S)-

There total 6 articles about Benzoic acid, 4-bromo-, 2-hydroxyheptyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Bromo-benzoic acid 2-oxo-heptyl ester (141339-61-9) → (S)-2-hydroxyheptyl 4-bromobenzoate (141339-69-7)

Guidance literature:

With D-glucose; immobilized baker's yeast; In water; at 35 ℃; for 72h; Yield given;

DOI:10.1246/bcsj.65.631

Reference yield:

1-chloro-2-heptanone (41055-92-9) → (S)-2-hydroxyheptyl 4-bromobenzoate (141339-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / tetrabutylammonium bromide / benzene / 3 h / Heating

2: immobilized baker's yeast, glucose / H₂O / 72 h / 35 °C

With D-glucose; immobilized baker's yeast; tetrabutylammomium bromide; In water; benzene;

DOI:10.1246/bcsj.65.631

Reference yield:

potassium 4-bromobenzoate (51550-68-6) → (S)-2-hydroxyheptyl 4-bromobenzoate (141339-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / tetrabutylammonium bromide / benzene / 3 h / Heating

2: immobilized baker's yeast, glucose / H₂O / 72 h / 35 °C

With D-glucose; immobilized baker's yeast; tetrabutylammomium bromide; In water; benzene;

DOI:10.1246/bcsj.65.631

upstream raw materials:

4-Bromo-benzoic acid 2-oxo-heptyl ester

1-chloro-2-heptanone

potassium 4-bromobenzoate

t-butyl 2-chloro-3-oxooctanoate