Cyclopropanecarboxylic acid, 3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)- 2-pentalenyl]-2,2-dimethyl-, methyl ester

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)- 2-pentalenyl]-2,2-dimethyl-, methyl ester
CAS No.:141422-40-4
Molecular Formula:C₂₇H₃₅NO₅
Molecular Weight:453.579
Hs Code.:
Mol file:141422-40-4.mol

Cyclopropanecarboxylic acid,
3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)-
2-pentalenyl]-2,2-dimethyl-, methyl ester

Synonyms:

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Chemical Property of Cyclopropanecarboxylic acid, 3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)- 2-pentalenyl]-2,2-dimethyl-, methyl ester

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Technology Process of Cyclopropanecarboxylic acid, 3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)- 2-pentalenyl]-2,2-dimethyl-, methyl ester

There total 5 articles about Cyclopropanecarboxylic acid, 3-[4-(benzoyloxy)-1,3a,4,5,6,6a-hexahydro-3a-methyl-3-(4-morpholinyl)- 2-pentalenyl]-2,2-dimethyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1120-73-6
2-methyl-2-cyclopenten-1-one

: 141422-40-4
Benzoic acid (3aR,6aR)-5-(3-methoxycarbonyl-2,2-dimethyl-cyclopropyl)-6a-methyl-6-morpholin-4-yl-1,2,3,3a,4,6a-hexahydro-pentalen-1-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: CuBr, Me₂S / tetrahydrofuran / 15 h / -78 °C

2: HCl / tetrahydrofuran / 24 h / 40 °C

3: 90 percent / pyridine / tetrahydrofuran / 4 h / 25 °C

4: 91 percent / pTsOH / ethylbenzene / 24 h / Heating

With pyridine; hydrogenchloride; dimethylsulfide; toluene-4-sulfonic acid; copper(I) bromide; In tetrahydrofuran; ethylbenzene;
DOI:10.1016/S0040-4039(00)99431-0

Reference yield:

: 102971-48-2,125184-80-7,125184-85-2
(3aR,6aS)-6-Hydroxy-6a-methyl-hexahydro-pentalen-1-one

: 141422-40-4
Benzoic acid (3aR,6aR)-5-(3-methoxycarbonyl-2,2-dimethyl-cyclopropyl)-6a-methyl-6-morpholin-4-yl-1,2,3,3a,4,6a-hexahydro-pentalen-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / tetrahydrofuran / 4 h / 25 °C

2: 91 percent / pTsOH / ethylbenzene / 24 h / Heating

With pyridine; toluene-4-sulfonic acid; In tetrahydrofuran; ethylbenzene;
DOI:10.1016/S0040-4039(00)99431-0

Reference yield:

: 125196-76-1,141422-35-7
(2R,3S)-3-(2-[1,3]Dioxan-2-yl-ethyl)-2-methyl-cyclopentanone

: 141422-40-4
Benzoic acid (3aR,6aR)-5-(3-methoxycarbonyl-2,2-dimethyl-cyclopropyl)-6a-methyl-6-morpholin-4-yl-1,2,3,3a,4,6a-hexahydro-pentalen-1-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / tetrahydrofuran / 24 h / 40 °C

2: 90 percent / pyridine / tetrahydrofuran / 4 h / 25 °C

3: 91 percent / pTsOH / ethylbenzene / 24 h / Heating

With pyridine; hydrogenchloride; toluene-4-sulfonic acid; In tetrahydrofuran; ethylbenzene;
DOI:10.1016/S0040-4039(00)99431-0