Carbamic acid, [2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2 -oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)-

Base Information

Chemical Name:Carbamic acid, [2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2 -oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)-
CAS No.:141468-82-8
Molecular Formula:C₂₆H₂₈BrClN₂O₆
Molecular Weight:579.875
Hs Code.:
Mol file:141468-82-8.mol

Carbamic acid,
[2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2
-oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)-

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Chemical Property of Carbamic acid, [2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2 -oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)-

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Technology Process of Carbamic acid, [2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2 -oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)-

There total 1 articles about Carbamic acid, [2-[[3-(3-bromopropoxy)-4-chloro-1-oxo-1H-2-benzopyran-7-yl]amino]-2 -oxo-1-(phenylmethyl)ethyl]-, 1,1-dimethylethyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 113251-20-0
7-amino-3-(3-bromopropoxy)-4-chloroisocoumarin

: 88719-17-9
[Boc-D-Phe]2O

: 141468-82-8
{(R)-1-[3-(3-Bromo-propoxy)-4-chloro-1-oxo-1H-isochromen-7-ylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00003a017

Reference yield: 40.0%

: 17356-08-0
thiourea

: 141468-82-8
{(R)-1-[3-(3-Bromo-propoxy)-4-chloro-1-oxo-1H-isochromen-7-ylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

: 7-<<(tert-butoxycarbonyl)-D-phenylalanyl>amino>-4-chloro-3-(3-isothioureidopropoxy)isocoumarin hydrobromide

Guidance literature:: In tetrahydrofuran; Heating;
DOI:10.1021/jm00035a009

Reference yield:

: 141468-82-8
{(R)-1-[3-(3-Bromo-propoxy)-4-chloro-1-oxo-1H-isochromen-7-ylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

: 4-chloro-3-(3-isothioureidopropoxy)-7-(D-pheylalanylamino)-isocoumarin trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / tetrahydrofuran / Heating

2: 90 percent / 0.08 h / 0 °C

In tetrahydrofuran;
DOI:10.1021/jm00035a009