Technology Process of Benzoic acid, 4-[3-[(1-oxo-3-butenyl)oxy]propoxy]-, 4-cyanophenyl ester
There total 4 articles about Benzoic acid, 4-[3-[(1-oxo-3-butenyl)oxy]propoxy]-, 4-cyanophenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / p-TsOH, benzene-1,4-diol
2: SOCl2 / dimethylformamide
3: Et3N
With
thionyl chloride; toluene-4-sulfonic acid; triethylamine; hydroquinone;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: SOCl2 / dimethylformamide
2: Et3N
With
thionyl chloride; triethylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 81 percent / KOH, KI / ethanol; H2O
2: 63 percent / p-TsOH, benzene-1,4-diol
3: SOCl2 / dimethylformamide
4: Et3N
With
potassium hydroxide; thionyl chloride; toluene-4-sulfonic acid; triethylamine; hydroquinone; potassium iodide;
In
ethanol; water; N,N-dimethyl-formamide;
