4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

Base Information

Chemical Name:4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone
CAS No.:141621-90-1
Molecular Formula:C26H30O
Molecular Weight:358.524
Hs Code.:
Mol file:141621-90-1.mol

Synonyms:4-tert-Butyl-2,6-bis-[1-p-tolyl-meth-(E)-ylidene]-cyclohexanone;4-t-butyl-2,6-bis(p-methylbenzylidene)cyclohexanone;

Suppliers and Price of 4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

Chemical Property:

PSA：17.07000
LogP:6.79560

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

There total 1 articles about 4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 104-87-0
4-methyl-benzaldehyde

: 98-53-3
4-tercbutyl-cyclohexanone

: 141621-90-1
(2E,6E)-4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

Guidance literature:: With nano titania supported sulfonic acid; In neat (no solvent); at 90 ℃; for 0.5h; Green chemistry;
DOI:10.101.6/j.arabjc.2011.06.001

Reference yield: 92.0%

: 126-81-8
dimedone

: 141621-90-1
(2E,6E)-4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

: (E)-7-(tert-butyl)-3,3-dimethyl-5-(4-methylbenzylidene)-9-(p-tolyl)-2,3,4,5,6,7,8,9-octahydro-1H-xanthen-1-one

Guidance literature:: With nano titania supported sulfonic acid; In neat (no solvent); at 130 ℃; for 2.08333h; Green chemistry;
DOI:10.101.6/j.arabjc.2011.06.001

Reference yield: 77.0%

: 14369-81-4
ethyl 2,3-butadienoate

: 141621-90-1
(2E,6E)-4-tert-butyl-2,6-bis(4-methylbenzylidene)cyclohexanone

: 1263215-73-1
(E)-ethyl 9-tert-butyl-7-(4-methylbenzylidene)-6-oxo-4-p-tolylspiro[4.5]dec-1-ene-1-carboxylate

Guidance literature:: With (S,S)-FerroPHANE; In toluene; at 80 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc03164j