4-Oxazoleethanol, b-[1,3-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-phenyl-a-[(phen ylthio)methyl]-

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Chemical Name:4-Oxazoleethanol, b-[1,3-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-phenyl-a-[(phen ylthio)methyl]-
CAS No.:142075-63-6
Molecular Formula:C33H51NO4SSi2
Molecular Weight:614.009
Hs Code.:

Synonyms:

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Chemical Property of 4-Oxazoleethanol, b-[1,3-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-phenyl-a-[(phen ylthio)methyl]-

Chemical Property:

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Technology Process of 4-Oxazoleethanol, b-[1,3-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-phenyl-a-[(phen ylthio)methyl]-

There total 6 articles about 4-Oxazoleethanol, b-[1,3-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-phenyl-a-[(phen ylthio)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 142075-80-7
(3R,4S)-4,6-Bis-(tert-butyl-dimethyl-silanyloxy)-3-((S)-2-phenyl-4,5-dihydro-oxazol-4-yl)-1-phenylsulfanyl-hexan-2-ol

: 142075-63-6
(3R,4S)-4,6-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(2-phenyl-oxazol-4-yl)-1-phenylsulfanyl-hexan-2-ol

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; Heating;
DOI:10.1016/S0040-4039(00)79046-0

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 142075-63-6
(3R,4S)-4,6-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(2-phenyl-oxazol-4-yl)-1-phenylsulfanyl-hexan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Et₃N, 2) DIBAL / 1) CH₂Cl₂, -78 deg C, 2) CH₂Cl₂, -78 deg C

2: 40 percent / tetrahydrofuran / -78 °C

3: 100 percent / 2,3-dichloro-5,6-dicyanoquinone / benzene / Heating

With diisobutylaluminium hydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(00)79046-0

Reference yield:

: 89922-82-7
3-(tert-butyldimethylsilanyloxy)propionaldehyde

: 142075-63-6
(3R,4S)-4,6-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(2-phenyl-oxazol-4-yl)-1-phenylsulfanyl-hexan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) LiNEt₂ / 1) THF, -78 deg C, 2) -78 deg C

2: 1) Et₃N, 2) DIBAL / 1) CH₂Cl₂, -78 deg C, 2) CH₂Cl₂, -78 deg C

3: 40 percent / tetrahydrofuran / -78 °C

4: 100 percent / 2,3-dichloro-5,6-dicyanoquinone / benzene / Heating

With lithium diethylamide; diisobutylaluminium hydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(00)79046-0