(6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine

Base Information

• Chemical Name: (6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine
• CAS No.: 142138-64-5
• Molecular Formula: C₂₀H₁₆N₂
• Molecular Weight: 284.36
• DSSTox Substance ID: DTXSID70576540
• Mol file: 142138-64-5.mol

Synonyms:142138-64-5;(6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine;DTXSID70576540

Chemical Property of (6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 284.131348519
• Heavy Atom Count: 22
• Complexity: 410

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C2=CC=CC=C2C3=CC=CC=C3C1=NC4=CC=CC=C4

Technology Process of (6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine

There total 2 articles about (6Z)-5-Methyl-N-phenylphenanthridin-6(5H)-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C20H17N2(1+)*CH3O4S(1-) → 5-methyl-6-phenylamino-5,6-dihydrophenanthridine (142138-64-5)

Guidance literature:

With ammonium hydroxide;

DOI:10.1007/BF00486804

Reference yield: 83.0%

6-anilinophenanthridine (846-62-8) + dimethyl sulfate (77-78-1) → 5-methyl-6-phenylamino-5,6-dihydrophenanthridine (142138-64-5)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1007/BF00767009

upstream raw materials:

6-anilinophenanthridine

dimethyl sulfate