1,2-Dihydrobenz(e)aceanthrylene

Base Information

Chemical Name:1,2-Dihydrobenz(e)aceanthrylene
CAS No.:3697-25-4
Molecular Formula:C20H14
Molecular Weight:254.34
Hs Code.:
UNII:A40GJ1T67K
DSSTox Substance ID:DTXSID90190464
Wikidata:Q27273592

Synonyms:Benz(e)aceanthrene;1,2-Dihydrobenz(e)aceanthrylene;4,10-Ace-1,2-benzanthracene;BRN 3609984;A40GJ1T67K;BENZ(e)ACEANTHRYLENE, 5,6-DIHYDRO-;3697-25-4;UNII-A40GJ1T67K;DTXSID90190464;LS-24784;4,10-DIMETHYLENE-1,2-BENZANTHRACENE;CYCLOPENTA(GH)BENZ(A)ANTHRACENE, 5,6-DIHYDRO-;Q27273592

Suppliers and Price of 1,2-Dihydrobenz(e)aceanthrylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,2-Dihydrobenz(e)aceanthrylene

Chemical Property:

Vapor Pressure:5.74E-12mmHg at 25°C
Boiling Point:559.3°Cat760mmHg
Flash Point:338.8°C
Density:1.25g/cm³
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:254.109550447
Heavy Atom Count:20
Complexity:557

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=C2C(=C1)C=C3C=CC4=C3C2=CC5=CC=CC=C45

Technology Process of 1,2-Dihydrobenz(e)aceanthrylene

There total 4 articles about 1,2-Dihydrobenz(e)aceanthrylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 127229-54-3
1,2,9,10,11,12-Hexahydrobenzaceanthrylene

: 3697-25-4
1,2-Dihydrobenzaceanthrylene

Guidance literature:: palladium on activated charcoal; In various solvent(s); for 2h; Heating;
DOI:10.1021/jo00299a018

Reference yield:

: 127229-50-9
Ethyl (7-benz anthracenyl) acetate

: 3697-25-4
1,2-Dihydrobenzaceanthrylene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 1034.3 Torr

2: 76 percent / HF / 12 h

3: 73 percent / H₂NNH₂, KOH / ethane-1,2-diol / 12 h / Heating

4: 95 percent / 10percent Pd/C / various solvent(s) / 2 h / Heating

With potassium hydroxide; hydrogen fluoride; hydrogen; hydrazine; platinum(IV) oxide; palladium on activated charcoal; In ethylene glycol; ethyl acetate;
DOI:10.1021/jo00299a018

Reference yield:

: 127229-53-2
2-Oxo-1,2,9,10,11,12-hexahydrobenzaceanthrylene

: 3697-25-4
1,2-Dihydrobenzaceanthrylene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / H₂NNH₂, KOH / ethane-1,2-diol / 12 h / Heating

2: 95 percent / 10percent Pd/C / various solvent(s) / 2 h / Heating

With potassium hydroxide; hydrazine; palladium on activated charcoal; In ethylene glycol;
DOI:10.1021/jo00299a018