N-Benzoyl-N,2-dimethylbenzamide

Base Information

Chemical Name:N-Benzoyl-N,2-dimethylbenzamide
CAS No.:142338-01-0
Molecular Formula:C16H15NO2
Molecular Weight:253.301
Hs Code.:
DSSTox Substance ID:DTXSID10570865
Wikidata:Q82458430

Synonyms:N-Benzoyl-N,2-dimethylbenzamide;142338-01-0;DTXSID10570865

Suppliers and Price of N-Benzoyl-N,2-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-Benzoyl-N,2-dimethylbenzamide

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:253.110278721
Heavy Atom Count:19
Complexity:334

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(=O)N(C)C(=O)C2=CC=CC=C2

Technology Process of N-Benzoyl-N,2-dimethylbenzamide

There total 6 articles about N-Benzoyl-N,2-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 2170-09-4
N,2-dimethylbenzamide

: 108-88-3,15644-74-3,16713-13-6
toluene

: 142338-01-0
N-benzoyl-N,2-dimethylbenzamide

Guidance literature:: With tert.-butylhydroperoxide; water; iodine; sodium carbonate; In neat (no solvent); at 110 ℃; for 20h; Sealed tube;
DOI:10.1021/acs.orglett.6b01684

Reference yield:

: 188674-64-8
N-[2-(Bis-trimethylsilanyl-methyl)-benzoyl]-N-methyl-benzamide

: 34497-10-4
2-methyl-3-phenylisoquinolin-1(2H)-one

: 142338-01-0
N-benzoyl-N,2-dimethylbenzamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.0833333h; under 0.05 Torr; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1039/a605077h

Reference yield:

: 2170-09-4
N,2-dimethylbenzamide

: 142338-01-0
N-benzoyl-N,2-dimethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: BuLi / tetrahydrofuran / 1.) -78 deg C, 0.5 h, 2.) -78 deg C, 1 h

2: BuLi / tetrahydrofuran / 1.) -78 deg C, 0.5 h, 2.) -78 deg C to r.t.

3: BuLi / tetrahydrofuran / 1.) 0 deg C, 2.) r.t., 1 h

4: TBAF / tetrahydrofuran / 0.08 h / 0.05 Torr / Ambient temperature

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1039/a605077h