Technology Process of 3-Thiopheneheptanoic acid, 5-(3-phenylpropyl)-
There total 4 articles about 3-Thiopheneheptanoic acid, 5-(3-phenylpropyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrazine hydrate;
In
various solvent(s);
at 210 ℃;
for 4h;
DOI:10.1021/jm00095a011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92.8 percent / N-bromosuccinimide / ethyl acetate; CHCl3 / 0.03 h
2: 61 percent / SnCl4 / 1,2-dichloro-ethane / 1 h / Ambient temperature
3: 50 percent / Zn, acetic acid / H2O / 24 h / Ambient temperature
4: 92 percent / H2NNH2*H20, KOH / various solvent(s) / 4 h / 210 °C
With
potassium hydroxide; N-Bromosuccinimide; tin(IV) chloride; hydrazine hydrate; acetic acid; zinc;
In
chloroform; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/jm00095a011
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 61 percent / SnCl4 / 1,2-dichloro-ethane / 1 h / Ambient temperature
2: 50 percent / Zn, acetic acid / H2O / 24 h / Ambient temperature
3: 92 percent / H2NNH2*H20, KOH / various solvent(s) / 4 h / 210 °C
With
potassium hydroxide; tin(IV) chloride; hydrazine hydrate; acetic acid; zinc;
In
water; 1,2-dichloro-ethane;
DOI:10.1021/jm00095a011