Technology Process of Thiophene, 2-(5-bromopentyl)-3-(3-phenylpropyl)-
There total 5 articles about Thiophene, 2-(5-bromopentyl)-3-(3-phenylpropyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
allyl bromide; 1,1'-carbonyldiimidazole;
In
acetonitrile;
for 2h;
Heating;
DOI:10.1021/jm00095a011
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 76 percent / H2NNH2*H2O, KOH / various solvent(s) / 4 h / 210 °C
2: SnCl4 / 1,2-dichloro-ethane / 1 h / Ambient temperature
3: H2NNH2*H2O, KOH / various solvent(s) / 4 h / 210 °C
4: 76 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
5: 89 percent / 1,1'-carbonyldiimidazole, allyl bromide / acetonitrile / 2 h / Heating
With
potassium hydroxide; lithium aluminium tetrahydride; tin(IV) chloride; hydrazine hydrate; allyl bromide; 1,1'-carbonyldiimidazole;
In
diethyl ether; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jm00095a011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: SnCl4 / 1,2-dichloro-ethane / 1 h / Ambient temperature
2: H2NNH2*H2O, KOH / various solvent(s) / 4 h / 210 °C
3: 76 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
4: 89 percent / 1,1'-carbonyldiimidazole, allyl bromide / acetonitrile / 2 h / Heating
With
potassium hydroxide; lithium aluminium tetrahydride; tin(IV) chloride; hydrazine hydrate; allyl bromide; 1,1'-carbonyldiimidazole;
In
diethyl ether; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jm00095a011