11-Oxa-2,4,9-triazatridec-2-enoic acid, 8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl] amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester

Base Information

Chemical Name:11-Oxa-2,4,9-triazatridec-2-enoic acid, 8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl] amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester
CAS No.:142801-56-7
Molecular Formula:C27H44N4O10S
Molecular Weight:616.733
Hs Code.:

11-Oxa-2,4,9-triazatridec-2-enoic acid,
8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl]
amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester

Synonyms:

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Chemical Property of 11-Oxa-2,4,9-triazatridec-2-enoic acid, 8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl] amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester

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Technology Process of 11-Oxa-2,4,9-triazatridec-2-enoic acid, 8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl] amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester

There total 4 articles about 11-Oxa-2,4,9-triazatridec-2-enoic acid, 8-(carboxyhydroxymethyl)-3-[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl] amino]-12,12-dimethyl-10-oxo-, 1-(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 142801-56-7
(S)-3-tert-Butoxycarbonylamino-6-{[[(Z)-tert-butoxycarbonylimino]-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-amino}-2-hydroxy-hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DMAP

2: LiAlH₄ / tetrahydrofuran

3: 1.) n-BuLi, 2.) HgO, HgCl₂, H₂O, 3.) aq. LiOH

With dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; water; mercury dichloride; mercury(II) oxide; In tetrahydrofuran;
DOI:10.1021/ja00042a053

Reference yield:

: 142801-55-6
N-α-(t-butyloxycarbonyl)-N'-ω'-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-L-arginine-N,O-dimethylhydroxyamide

: 142801-56-7
(S)-3-tert-Butoxycarbonylamino-6-{[[(Z)-tert-butoxycarbonylimino]-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-amino}-2-hydroxy-hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DMAP

2: LiAlH₄ / tetrahydrofuran

3: 1.) n-BuLi, 2.) HgO, HgCl₂, H₂O, 3.) aq. LiOH

With dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; water; mercury dichloride; mercury(II) oxide; In tetrahydrofuran;
DOI:10.1021/ja00042a053

Reference yield:

: 183442-79-7
[(S)-4-{[[(Z)-tert-Butoxycarbonylimino]-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-amino}-1-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester

: 142801-56-7
(S)-3-tert-Butoxycarbonylamino-6-{[[(Z)-tert-butoxycarbonylimino]-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-amino}-2-hydroxy-hexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

2: 1.) n-BuLi, 2.) HgO, HgCl₂, H₂O, 3.) aq. LiOH

With lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; water; mercury dichloride; mercury(II) oxide; In tetrahydrofuran;
DOI:10.1021/ja00042a053