1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE

Base Information

Chemical Name:1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE
CAS No.:142868-94-8
Molecular Formula:C9H18Cl2S2
Molecular Weight:261.27500
Hs Code.:
Mol file:142868-94-8.mol

Synonyms:1,5-bis-(2-chloro-ethylsulfanyl)-pentane;Pentane,1,5-bis((2-chloroethyl)thio);1,5-Bis-(2-chlor-aethylmercapto)-pentan;1,5-bis(2-chloroethylthio)pentane;

Suppliers and Price of 1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:358.908oC at 760 mmHg
Flash Point:160.472oC
PSA：50.60000
LogP:4.10070

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE

There total 3 articles about 1,5-BIS(2-CHLOROETHYLTHIO)-N-PENTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5400-84-0
1,5-bis(2-hydroxyethylthio)pentane

: 142868-94-8
bis-1,5-(20chloroethylthio)pentane

Guidance literature:: With thionyl chloride; diethyl ether;
DOI:10.1021/ja01197a055

Reference yield:

: 928-98-3
pentane-1,5-dithiol

: 142868-94-8
bis-1,5-(20chloroethylthio)pentane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / ethanol / 1 h / Inert atmosphere; Heating; Schlenk technique

1.2: 1.5 h / 20 °C / Reflux; Inert atmosphere; Schlenk technique

2.1: thionyl chloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With thionyl chloride; sodium; In ethanol; dichloromethane;
DOI:10.1021/acs.joc.8b01670

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 142868-94-8
bis-1,5-(20chloroethylthio)pentane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethylate

2: chloroform; SOCl₂

With thionyl chloride; chloroform; sodium ethanolate;