2H-Isoindole-1-carboxylic acid, 3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4,5,6,7-tetrahydro-, phenylmethyl ester

Base Information

Chemical Name:2H-Isoindole-1-carboxylic acid, 3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4,5,6,7-tetrahydro-, phenylmethyl ester
CAS No.:143064-86-2
Molecular Formula:C₂₉H₃₆N₂O₄
Molecular Weight:476.616
Hs Code.:

2H-Isoindole-1-carboxylic acid,
3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth
yl]-4,5,6,7-tetrahydro-, phenylmethyl ester

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Chemical Property of 2H-Isoindole-1-carboxylic acid, 3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4,5,6,7-tetrahydro-, phenylmethyl ester

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Technology Process of 2H-Isoindole-1-carboxylic acid, 3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4,5,6,7-tetrahydro-, phenylmethyl ester

There total 5 articles about 2H-Isoindole-1-carboxylic acid, 3-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4,5,6,7-tetrahydro-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34549-93-4
ethyl 3-ethyl-4,5-dimethylpyrrole-2-carboxylate

: 143064-86-2
benzyl 3,4-butano-5'-(tert-butoxycarbonyl)-4'-ethyl-3'-methyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / aq.NaOH / methanol / 4 h / Heating

2: 1) methanolic NaOH, 2) oxalyl chloride / 2) benzene, r.t., 1 h

3: NEt₃ / benzene / 0.5 h

4: 87 percent / HOAc / 2 h

5: Montmorillonite clay K₁₀ / 1 h

With sodium hydroxide; oxalyl dichloride; Montmorillonite clay K₁₀; acetic acid; triethylamine; In methanol; benzene;
DOI:10.1021/jo00044a013

Reference yield:

: 1026747-57-8
3-Ethyl-4,5-dimethyl-1H-pyrrole-2-carbonyl chloride

: 143064-86-2
benzyl 3,4-butano-5'-(tert-butoxycarbonyl)-4'-ethyl-3'-methyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃ / benzene / 0.5 h

2: 87 percent / HOAc / 2 h

3: Montmorillonite clay K₁₀ / 1 h

With Montmorillonite clay K₁₀; acetic acid; triethylamine; In benzene;
DOI:10.1021/jo00044a013

Reference yield:

: 65880-17-3
ethyl 4,5,6,7-tetrahydro-2H-isoindole-1-carboxylate

: 143064-86-2
benzyl 3,4-butano-5'-(tert-butoxycarbonyl)-4'-ethyl-3'-methyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Na / 2) boiling water-bath, 6 h

2: Montmorillonite clay K₁₀ / 1 h

With Montmorillonite clay K₁₀; sodium;
DOI:10.1021/jo00044a013