Perylene, 3,10-diphenyl-

Base Information

Chemical Name:Perylene, 3,10-diphenyl-
CAS No.:143076-97-5
Molecular Formula:C32H20
Molecular Weight:404.511
Hs Code.:
Mol file:143076-97-5.mol

Synonyms:

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Chemical Property of Perylene, 3,10-diphenyl-

Chemical Property:

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Technology Process of Perylene, 3,10-diphenyl-

There total 4 articles about Perylene, 3,10-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 198-55-0
PERYLENE

: 98-80-6
phenylboronic acid

: 3,9-diphenylperylene

: 143076-97-5
3,10-diphenylperylene

Guidance literature:: PERYLENE; With bromine; acetic acid; at 40 ℃; for 4h;

phenylboronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; at 90 ℃; for 60h; Overall yield = 92 %; Overall yield = 1.1 g;

Reference yield:

: 49610-35-7
4,4'-dibromo-1,1'-binaphthyl

: 143076-97-5
3,10-diphenylperylene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. 2 N K₂CO₃ / tetrakis(triphenylphosphane)palladium⁽⁰⁾ / toluene; butan-1-ol / 48 h / Heating

2: 1.) potassium, 2.) cadmium chloride / 1.) 1,2-dimethoxyethane, room temperature, 3 d, 2.) room temperature, 1 h

With potassium; potassium carbonate; cadmium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; butan-1-ol;

Reference yield:

: 98-80-6
phenylboronic acid

: 143076-97-5
3,10-diphenylperylene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. 2 N K₂CO₃ / tetrakis(triphenylphosphane)palladium⁽⁰⁾ / toluene; butan-1-ol / 48 h / Heating

2: 1.) potassium, 2.) cadmium chloride / 1.) 1,2-dimethoxyethane, room temperature, 3 d, 2.) room temperature, 1 h

With potassium; potassium carbonate; cadmium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; butan-1-ol;