endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol

Base Information

Chemical Name:endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol
CAS No.:16423-26-0
Molecular Formula:C₁₁H₂₀O
Molecular Weight:168.279
Hs Code.:
Mol file:16423-26-0.mol

Synonyms:2-Norbornaneethanol,3,3-dimethyl-, endo- (8CI); Bicyclo[2.2.1]heptane-2-ethanol, 3,3-dimethyl-,endo-

Suppliers and Price of endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol

Chemical Property:

Boiling Point:234.5°Cat760mmHg
Flash Point:103.8°C
PSA：20.23000
Density:0.941g/cm³
LogP:2.44110

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol

There total 8 articles about endo-2-[3,3-dimethylbicyclo[2.2.1]hept-2-yl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3,3-Dimethyl-bicyclo<2.2.1>hept-2-yl-essigsaeuremethylester

: 2226-08-6,16423-26-0,16503-26-7,130857-70-4,130857-71-5
2-(3,3-Dimethyl-bicyclo<2.2.1>hept-2-yl)-ethanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;
DOI:10.1007/BF00809157

Reference yield:

: 131131-58-3
endo-3,3-Dimethylbicyclo<2.2.1>heptane-2-acetic acid

: 2226-08-6,16423-26-0,16503-26-7,130857-70-4,130857-71-5
2-(3,3-Dimethyl-bicyclo<2.2.1>hept-2-yl)-ethanol

Guidance literature:: With lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/ja01128a073

Reference yield:

: 18310-55-9,18410-94-1,27899-45-2,63373-82-0,67560-14-9,72188-57-9,81601-68-5,81601-70-9,105453-57-4
endo-2,2-dimethyl-3-hydroxymethylbicyclo<2.2.1>heptane

: 2226-08-6,16423-26-0,16503-26-7,130857-70-4,130857-71-5
2-(3,3-Dimethyl-bicyclo<2.2.1>hept-2-yl)-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / pyridine / 15 min, -5 deg C, then room temp., overnight

2: 61 percent / dimethylsulfoxide / 6 h / 100 - 120 °C

3: 90 percent / KOH / ethane-1,2-diol / 24 h / Heating

5: 80 percent / LiAlH₄ / diethyl ether / 1 h / Heating

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; In diethyl ether; ethylene glycol; dimethyl sulfoxide;
DOI:10.1007/BF00809157