1H-Imidazole, 1-(3-butynyl)-2-nitro-

Base Information

Chemical Name:1H-Imidazole, 1-(3-butynyl)-2-nitro-
CAS No.:143334-79-6
Molecular Formula:C7H7N3O2
Molecular Weight:165.151
Hs Code.:
Mol file:143334-79-6.mol

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Chemical Property of 1H-Imidazole, 1-(3-butynyl)-2-nitro-

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Technology Process of 1H-Imidazole, 1-(3-butynyl)-2-nitro-

There total 1 articles about 1H-Imidazole, 1-(3-butynyl)-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 527-73-1
2-nitro-1H-imidazole

: 23418-85-1
3-butyn-1-yl p-toluenesulfonate

: 143334-79-6
1-(CHC(CH₂)2)-2-nitroimidazole

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; at 130 ℃; for 0.166667h;
DOI:10.1039/P19940000203

Reference yield: 57.0%

: 1-{4-(hydroxyiminomethyl)phenoxymethyl}-1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 143334-79-6
1-(CHC(CH₂)2)-2-nitroimidazole

: C₁₇H₂₆B₁₀N₄O₄

: 143334-76-3
4-(1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-ylmethoxy)benzonitrile N-oxide

Guidance literature:: With NaOCl; H₂O; In dichloromethane; vigorous stirring of the oxime and the alkyne in CH2Cl2 together with aq. NaOCl for 18 h, addn. of further aq. NaOCl, stirring for a further 1.5 h; washing (H2O), evapn., chromy. of the residue (silica gel, pentane-CH2Cl2 1:1, then CH2Cl2, then CH2Cl2-diethyl ether 2:1), from the first fraction: the N-oxide, from the third fraction: the imidazole;
DOI:10.1039/P19940000203

Reference yield:

: C₂B₁₀H₁₀CH₂OC₆H₄CHNOH

: 143334-79-6
1-(CHC(CH₂)2)-2-nitroimidazole

: (C₂B₁₀H₁₀)CH₂OC₆H₄(C₃NOH₃)C₂H₄(C₃N₂H₂(NO₂))

Guidance literature:: With sodium hypochlorite; In dichloromethane; the oxime and the imidazole in CH2Cl2 is treated with aq. NaOCl for 18 h; chromy. on silica gel, evapn.;
DOI:10.1039/c39920000939