1-Ethynyl-2-(phenylsulfanyl)benzene

Base Information

Chemical Name:1-Ethynyl-2-(phenylsulfanyl)benzene
CAS No.:143392-32-9
Molecular Formula:C14H10S
Molecular Weight:210.299
Hs Code.:
DSSTox Substance ID:DTXSID00566494
Wikidata:Q82452129
Mol file:143392-32-9.mol

Synonyms:1-Ethynyl-2-(phenylsulfanyl)benzene;143392-32-9;DTXSID00566494

Suppliers and Price of 1-Ethynyl-2-(phenylsulfanyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Ethynyl-2-(phenylsulfanyl)benzene

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:210.05032149
Heavy Atom Count:15
Complexity:231

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC1=CC=CC=C1SC2=CC=CC=C2

Technology Process of 1-Ethynyl-2-(phenylsulfanyl)benzene

There total 4 articles about 1-Ethynyl-2-(phenylsulfanyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 143521-46-4
1-phenyl-1-benzothiophenium trifluoromethanesulfonate

: 143392-32-9
(phenyl)(2-(ethynyl)phenyl)sulfane

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1246/cl.1992.1357

Reference yield:

: C₁₇H₁₈SSi

: 143392-32-9
(phenyl)(2-(ethynyl)phenyl)sulfane

Guidance literature:: With methanol; potassium carbonate; for 0.166667h;
DOI:10.1002/anie.201403796

Reference yield:

: 139-66-2
diphenyl sulfide

: 143392-32-9
(phenyl)(2-(ethynyl)phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2 h / -78 °C

2.1: potassium carbonate; methanol / 0.17 h

With methanol; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane;
DOI:10.1002/anie.201403796