Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-

Base Information

Chemical Name:Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-
CAS No.:143399-68-2
Molecular Formula:C14H16ClN
Molecular Weight:233.741
Hs Code.:
DSSTox Substance ID:DTXSID00437554
Mol file:143399-68-2.mol

Synonyms:Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-;143399-68-2;DTXSID00437554

Suppliers and Price of Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:233.0971272
Heavy Atom Count:16
Complexity:254

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=CN=CC2=CC=C(C=C2)Cl)CC1

Technology Process of Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene-

There total 2 articles about Methanamine, N-[(4-chlorophenyl)methylene]-1-cyclohexylidene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 143399-66-0
N-<(1-Chlorocyclohexyl)methylidene>-4-chlorobenzylamine

: 143399-68-2
N-(4-Chlorobenzylidene)cyclohexylidenemethylamine

Guidance literature:: With tert-butoxide; In diethyl ether; Ambient temperature;
DOI:10.1021/jo00047a034

Reference yield:

: 53627-10-4
1-chlorocyclohexane-1-carbaldehyde

: 143399-68-2
N-(4-Chlorobenzylidene)cyclohexylidenemethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

2: 80 percent / tert-butoxide / diethyl ether / Ambient temperature

With tert-butoxide; magnesium sulfate; In diethyl ether; dichloromethane;
DOI:10.1021/jo00047a034