1,4-Benzenedicarboxamide, 3-[(chloroacetyl)amino]-2,5-dimethoxy-N,N'-dimethyl-

Base Information

Chemical Name:1,4-Benzenedicarboxamide, 3-[(chloroacetyl)amino]-2,5-dimethoxy-N,N'-dimethyl-
CAS No.:143430-50-6
Molecular Formula:C14H18ClN3O5
Molecular Weight:343.767
Hs Code.:

Synonyms:

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Chemical Property of 1,4-Benzenedicarboxamide, 3-[(chloroacetyl)amino]-2,5-dimethoxy-N,N'-dimethyl-

Chemical Property:

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Technology Process of 1,4-Benzenedicarboxamide, 3-[(chloroacetyl)amino]-2,5-dimethoxy-N,N'-dimethyl-

There total 8 articles about 1,4-Benzenedicarboxamide, 3-[(chloroacetyl)amino]-2,5-dimethoxy-N,N'-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5628-41-1
3,6-dicyano-1,4-dimethoxy-2-nitrobenzene

: 143430-50-6
2-(chloroacetamido)-1,4-bis(methylcarbamyl)-3,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / 1 N aq. NaOH, 10percent aq. hydrogen peroxide / ethanol / 0.33 h / 40 °C

2: 73 percent / conc. sulfuric acid, aq. sodium nitrite / 70 °C

3: 75 percent / conc. sulfuric acid / Heating

4: 91 percent / methanol / 5 h / Ambient temperature

5: 75 percent / H₂ / 5percent Pd/C / methanol / 2585.7 Torr

6: 144 mg / pyridine / dimethylformamide / 2 h / Ambient temperature

With pyridine; sodium hydroxide; sulfuric acid; hydrogen; dihydrogen peroxide; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00047a017

Reference yield:

: 4655-68-9
2,5-Dimethoxy-1,4-benzoldicarbonitril

: 143430-50-6
2-(chloroacetamido)-1,4-bis(methylcarbamyl)-3,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 7 steps

1: 71 percent / acetic anhydride, 90percent nitric acid / 0.25 h / Ambient temperature

2: 80 percent / 1 N aq. NaOH, 10percent aq. hydrogen peroxide / ethanol / 0.33 h / 40 °C

3: 73 percent / conc. sulfuric acid, aq. sodium nitrite / 70 °C

4: 75 percent / conc. sulfuric acid / Heating

5: 91 percent / methanol / 5 h / Ambient temperature

6: 75 percent / H₂ / 5percent Pd/C / methanol / 2585.7 Torr

7: 144 mg / pyridine / dimethylformamide / 2 h / Ambient temperature

With pyridine; sodium hydroxide; sulfuric acid; hydrogen; dihydrogen peroxide; nitric acid; acetic anhydride; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00047a017

Reference yield:

: 143430-18-6
3,6-dicarbamyl-1,4-dimethoxy-2-nitrobenzene

: 143430-50-6
2-(chloroacetamido)-1,4-bis(methylcarbamyl)-3,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / conc. sulfuric acid, aq. sodium nitrite / 70 °C

2: 75 percent / conc. sulfuric acid / Heating

3: 91 percent / methanol / 5 h / Ambient temperature

4: 75 percent / H₂ / 5percent Pd/C / methanol / 2585.7 Torr

5: 144 mg / pyridine / dimethylformamide / 2 h / Ambient temperature

With pyridine; sulfuric acid; hydrogen; sodium nitrite; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00047a017