10-(2-Chlorobenzylidene)-9-anthrone

Base Information

Chemical Name:10-(2-Chlorobenzylidene)-9-anthrone
CAS No.:14343-94-3
Molecular Formula:C21H13ClO
Molecular Weight:316.787
Hs Code.:
European Community (EC) Number:665-854-4
Nikkaji Number:J2.045.744I
ChEMBL ID:CHEMBL155858
Mol file:14343-94-3.mol

Synonyms:10-(2-CHLOROBENZYLIDENE)-9-ANTHRONE;CHEMBL155858;AKOS024334825;9-(2-Chlorobenzylidene)anthracen-10(9H)-one;10-(2-Chlorobenzylidene)-9,10-dihydroanthracene-9-one

Suppliers and Price of 10-(2-Chlorobenzylidene)-9-anthrone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
10-(2-CHLOROBENZYLIDENE)-9-ANTHRONE AldrichCPR
250mg
$ 57.00

American Custom Chemicals Corporation
10-(2-CHLOROBENZYLIDENE)-9-ANTHRONE 95.00%
5MG
$ 504.67

Total 1 raw suppliers

Chemical Property of 10-(2-Chlorobenzylidene)-9-anthrone

Chemical Property:

PSA：17.07000
LogP:5.47330
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:316.0654927
Heavy Atom Count:23
Complexity:454

Purity/Quality:

98%,99%, ^*data from raw suppliers

10-(2-CHLOROBENZYLIDENE)-9-ANTHRONE AldrichCPR ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=C2C3=CC=CC=C3C(=O)C4=CC=CC=C42)Cl

Technology Process of 10-(2-Chlorobenzylidene)-9-anthrone

There total 1 articles about 10-(2-Chlorobenzylidene)-9-anthrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.5%

: 90-44-8
anthracen-9(10H)-one

: 89-98-5
2-chloro-benzaldehyde

: 14343-94-3
10-(2-chloro-benzyliden)-anthrone

Guidance literature:: With piperidine; pyridine; 4-methoxy-phenol; for 6h; Heating;
DOI:10.1016/j.bmcl.2003.11.053

Reference yield: 87.0%

: 107-97-1,25951-24-0
sarcosine

: 14343-94-3
10-(2-chloro-benzyliden)-anthrone

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: (2′S,4′S)-1′-methyl-4′-(2-chlorophenyl)-10H-dispiro[anthracene-9,3′-pyrrolidine-2′,3′′-indoline]-2′′,10-dione

Guidance literature:: With 1-n-butyl-3-methylimidazolim bromide; at 100 ℃; for 2h; regioselective reaction;
DOI:10.3390/molecules200916142

Reference yield:

: 14343-94-3
10-(2-chloro-benzyliden)-anthrone

: 14659-79-1
10-Benzyliden-9-(2-chlor-benzyliden)-9,10-dihydro-anthracen

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, Et₂O, (ii) /BRN= 2591181/

2: Ac₂O

With acetic anhydride;
DOI:10.1016/S0040-4020(01)82179-7