Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)-

Base Information

Chemical Name:Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)-
CAS No.:29890-04-8
Molecular Formula:C30H24 Cr O4 P2
Molecular Weight:562.462
Hs Code.:

Synonyms:Chromium,tetracarbonyl[1,2-ethanediylbis[diphenylphosphine-kP]]-, (OC-6-22)- (9CI); Chromium,tetracarbonyl[1,2-ethanediylbis[diphenylphosphine]-P,P']-, (OC-6-22)-;Chromium, tetracarbonyl[ethylenebis[diphenylphosphine]]- (7CI); Chromium,tetracarbonyl[ethylenebis[diphenylphosphine]]-, cis- (8CI); Phosphine,1,2-ethanediylbis[diphenyl-, chromium complex;Bis-1,2-diphenylphosphinoethanetetracarbonylchromium; NSC 193742;cis-Tetracarbonyl[ethylenebis[diphenylphosphine]]chromium

Suppliers and Price of Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)-

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)-

There total 13 articles about Chromium,tetracarbonyl[1,1'-(1,2-ethanediyl)bis[1,1-diphenylphosphine-kP]]-, (OC-6-22)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 29890-04-8
[1,2-bis(diphenylphosphino)ethane]chromium(0) tetracarbonyl

Guidance literature:: With sodium tetrahydroborate; at 110 ℃; for 0.333333h; under 760.051 Torr; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1016/j.inoche.2012.09.030

Reference yield: 90.0%

: 13007-92-6,199620-14-9
chromium hexacarbonyl

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 29890-04-8
cis-[Cr(CO)4(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: With sodium tetrahydroborate; at 110 ℃; for 0.333333h; under 760.051 Torr; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1016/j.inoche.2012.09.030

Reference yield: 90.0%

: 70568-68-2
cis-Cr(CO)4(PPh₂H)(PPh₂CHCH₂)

: 29890-04-8
[1,2-bis(diphenylphosphino)ethane]chromium(0) tetracarbonyl

Guidance literature:: With hydrogenchloride; phenyllithium; In tetrahydrofuran; N2-atmosphere; addn. of PhLi to soln. of Cr-complex, stirring (room temp., 2 h), addn. of 6 M soln. of HCl, 15 min; solvent removal (vac.), dissoln. (CHCl3), drying (over MgSO4), filtration, volume reduction, chromy. (CHCl3), solvent removal, crystn. (CH2Cl2/pentane);
DOI:10.1016/S0020-1693(00)89472-4