3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID

Base Information

• Chemical Name: 3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID
• CAS No.: 143610-62-2
• Molecular Formula: C8H8BrFO2
• Molecular Weight: 199.97200
• Mol file: 143610-62-2.mol

Synonyms:3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID;

Chemical Property of 3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID

Chemical Property:

• PSA: 58.92000
• LogP: -0.51180

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-2-fluoro-1-(methoxymethoxy)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID

There total 2 articles about 3-FLUORO-4-METHOXYMETHOXYPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-bromo-2-fluorophenol (2105-94-4) + chloromethyl methyl ether (107-30-2) → 4-bromo-2-fluoro-1-methoxymethoxybenzene (143610-62-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jm800839j

Reference yield: 96.0%

→ 4-bromo-2-fluoro-1-methoxymethoxybenzene (143610-62-2)

Guidance literature:

Reference yield: 71.0%

4-bromo-2-fluoro-1-methoxymethoxybenzene (143610-62-2) + trimethylsilylacetylene (1066-54-2) → 1-fluoro-2-methoxymethoxy-5-(2-trimethylsilylethynyl)benzene

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; In tetrahydrofuran; at 80 ℃; Inert atmosphere;

DOI:10.1246/cl.140779

upstream raw materials:

4-bromo-2-fluorophenol

chloromethyl methyl ether

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