Technology Process of 10H-Phenothiazine,
7-(1-methylethoxy)-10-[2-(1-methyl-2-piperidinyl)ethyl]-2-(methylsulfonyl)
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There total 6 articles about 10H-Phenothiazine,
7-(1-methylethoxy)-10-[2-(1-methyl-2-piperidinyl)ethyl]-2-(methylsulfonyl)
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guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: 70 percent / potassium carbonate / dimethylformamide / 20 h
2: 1.) sodium hydroxide / 1.) toluene, 7 h, 2.) toluene, reflux, 3 h
With
sodium hydroxide; potassium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570290455
- Guidance literature:
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Multi-step reaction with 6 steps
1: ethanol / 18 h / Ambient temperature
2: KOH / ethanol / 44 h
3: 1.) Zn, HCl, 2.) NaOH, O2 / 1.) CH3COOH, 60 deg C, 1 h, 2.) water, ethanol, 4 h
4: Na2S2O4 / H2O
5: 70 percent / potassium carbonate / dimethylformamide / 20 h
6: 1.) sodium hydroxide / 1.) toluene, 7 h, 2.) toluene, reflux, 3 h
With
hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium dithionite; oxygen; potassium carbonate; zinc;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570290455
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Zn, HCl, 2.) NaOH, O2 / 1.) CH3COOH, 60 deg C, 1 h, 2.) water, ethanol, 4 h
2: Na2S2O4 / H2O
3: 70 percent / potassium carbonate / dimethylformamide / 20 h
4: 1.) sodium hydroxide / 1.) toluene, 7 h, 2.) toluene, reflux, 3 h
With
hydrogenchloride; sodium hydroxide; sodium dithionite; oxygen; potassium carbonate; zinc;
In
water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570290455
