5-(Tributylstannyl)-1H-indole

Base Information

Chemical Name:5-(Tributylstannyl)-1H-indole
CAS No.:143724-34-9
Molecular Formula:C20H33NSn
Molecular Weight:408.20000
Hs Code.:2933299090
DSSTox Substance ID:DTXSID30577730
Mol file:143724-34-9.mol

Synonyms:5-(Tributylstannyl)-1H-indole;143724-34-9;1H-Indole, 5-(tributylstannyl)-;tributyl(1H-indol-5-yl)stannane;SCHEMBL7805665;DTXSID30577730;AKOS015839570

Suppliers and Price of 5-(Tributylstannyl)-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(TRIBUTYLSTANNYL)-1H-INDOLE 95.00%
5MG
$ 501.79

Total 3 raw suppliers

Chemical Property of 5-(Tributylstannyl)-1H-indole

Chemical Property:

PSA：12.03000
LogP:5.56100
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:407.163503
Heavy Atom Count:22
Complexity:282

Purity/Quality:

98%min ^*data from raw suppliers

5-(TRIBUTYLSTANNYL)-1H-INDOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CC2=C(C=C1)NC=C2

Technology Process of 5-(Tributylstannyl)-1H-indole

There total 3 articles about 5-(Tributylstannyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 10075-50-0
5-bromo-1H-indole

: 813-19-4
bis(tri-n-butyltin)

: 143724-34-9
5-(tributylstannyl)-1H-indole

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; at 110 ℃; for 3h; Reagent/catalyst; Inert atmosphere;
DOI:10.1021/ol302076d

Reference yield: 78.0%

: C₈H₅LiN^(1-)*K⁽¹⁺⁾

: 1461-22-9
tributyltin chloride

: 143724-34-9
5-(tributylstannyl)-1H-indole

Guidance literature:: In tetrahydrofuran; mineral oil; pentane; at -78 - 20 ℃;
DOI:10.1002/cmdc.201200316

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 143724-34-9
5-(tributylstannyl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

1.2: 0.33 h / -78 °C

2.1: tetrahydrofuran; mineral oil; pentane / -78 - 20 °C

With potassium hydride; In tetrahydrofuran; mineral oil; pentane;
DOI:10.1002/cmdc.201200316