Technology Process of 1,3-Benzenediacetic acid, 2,5-dimethoxy-4,6-bis(phenylseleno)-,
diethyl ester
There total 6 articles about 1,3-Benzenediacetic acid, 2,5-dimethoxy-4,6-bis(phenylseleno)-,
diethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide;
at 100 ℃;
for 3h;
DOI:10.1246/bcsj.65.1794
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Bu3P, aq. NaOH / 1.) THF, 15 min, 2.) THF, RT, 1 h
2: aq. Na2S2O4 / CH2Cl2
3: 1.) Ba(OH)2*8H2O / dimethylformamide
4: 52 percent / aq. LiCl / hexamethylphosphoric acid triamide / 3 h / 100 °C
With
barium dihydroxide; sodium hydroxide; sodium dithionite; tributylphosphine; lithium chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.65.1794
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) NaH / 1.) DMF, 4.5 h, 2.) DMF, 1 h
2: 1.) Bu3P, aq. NaOH / 1.) THF, 15 min, 2.) THF, RT, 1 h
3: aq. Na2S2O4 / CH2Cl2
4: 1.) Ba(OH)2*8H2O / dimethylformamide
5: 52 percent / aq. LiCl / hexamethylphosphoric acid triamide / 3 h / 100 °C
With
barium dihydroxide; sodium hydroxide; sodium dithionite; tributylphosphine; sodium hydride; lithium chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.65.1794
