2-[3-(4-methylphenyl)acryloyl]furan, 2-(4-Methylcinnamoyl)furan

Base Information

• Chemical Name: 2-[3-(4-methylphenyl)acryloyl]furan, 2-(4-Methylcinnamoyl)furan
• CAS No.: 14385-62-7
• Molecular Formula: C14H12O2
• Molecular Weight: 212.248
• Hs Code.: 2914399090
• Mol file: 14385-62-7.mol

Synonyms:1-(Fur-2-yl)-3-(4-methylphenyl)prop-2-en-1-one;1-(2-furyl)-3-(4-methylphenyl)prop-2-en-1-one;

Chemical Property of 2-[3-(4-methylphenyl)acryloyl]furan, 2-(4-Methylcinnamoyl)furan

Chemical Property:

• PSA: 30.21000
• LogP: 3.48410

Purity/Quality:

99% ^*data from raw suppliers

1-(Fur-2-yl)-3-(4-methylphenyl)prop-2-en-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[3-(4-methylphenyl)acryloyl]furan, 2-(4-Methylcinnamoyl)furan

There total 2 articles about 2-[3-(4-methylphenyl)acryloyl]furan, 2-(4-Methylcinnamoyl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(2-furyl)-1-ethanone (1192-62-7,80145-44-4) + 4-methyl-benzaldehyde (104-87-0) → 3-(4-methylphenyl)-1-(furan-2-yl)prop-2-en-1-one (14385-62-7)

Guidance literature:

With potassium fluoride modified clay; In methanol; at 20 ℃; for 0.333333h;

DOI:10.1134/S107042722007006X

Reference yield:

1-(2-furyl)-1-ethanone (1192-62-7,80145-44-4) + 4-chlorobenzaldehyde (104-88-1) → 3-(4-methylphenyl)-1-(furan-2-yl)prop-2-en-1-one (14385-62-7)

Guidance literature:

With I₂-neutral Al₂O₃; at 60 - 80 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1002/ardp.201200249

Reference yield: 99.0%

3-(4-methylphenyl)-1-(furan-2-yl)prop-2-en-1-one (14385-62-7) + ethyl acetoacetate (141-97-9) → ethyl 4-(furan-2-yl)-2-oxo-6-p-tolylcyclohex-3-enecarboxylate

Guidance literature:

With potassium carbonate; for 0.2h; Milling;

DOI:10.1007/s11164-015-2379-5

upstream raw materials:

1-(2-furyl)-1-ethanone

4-methyl-benzaldehyde

4-chlorobenzaldehyde

Downstream raw materials:

3-Furan-2-yl-5-p-tolyl-4,5-dihydro-1H-pyrazole

1-[3-(furan-2-yl)-4,5-dihydro-5-(4-methylphenyl)-pyrazol-1-yl]ethanone

3-Furan-2-yl-1-methyl-5-p-tolyl-4,5-dihydro-1H-pyrazole

C₂₀H₁₉N₃O₃S

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